2. Should be follow laboratory safety personal protective equipments while handling analysis.
3. Based on work allocation analysis should be perform and same day document completion.
4. All the analysis of raw materials, in-process, intermediate, stability, Recovery solvents, R&D
samples and finished product HPLC and GC analysis as per procedure.
5. All working standards HPLC and GC related analysis planned as per schedule date.
6. Working standard should be use by ensuring validity of standard within the period.
7. Chemist should be ensuring before using the instrument status and calibration of instrument
and earlier analysis results should be ensure.
8. Chemist should be ensure before starting analysis availability of standards, chemicals and
glasswares etc.,
9. Analyst should follow good laboratory practices laid down in the quality control laboratory.
10. Analyst should follow after completion of chromatography analysis ensure the results and
discard the solutions if results within the specification.
11. Analyst once started the sequence set of sample loading same day next day need to process
yesterday samples then only go for new work.
12. Analyst should process the samples contemporaneously if any abnormal results observed
inform immediately senior supervisor/reviewer/designee then only next decision to be taken.
13. Analyst is responsible for analysis and documentation and sample disposition.
14. Analyst is responsible for laboratory cleaning, instrument cleaning and maintenance in good
condition.
15. Results are reported as per rounding of the SOP.
16. Equipments calibration shall be performed as per internal calibration master schedule.
17. After usage of the working standards and reference standards it shall be kept in designated
place.
18. Monitoring the daily room temperature and its recording as per procedure.
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